Facilities
SerCon Elemental Analyser (Gas Solid / Liquid Preparation Unit)
Coupled with a 20-22 Stable Isotope Ratio Mass Spectrometer (Sercon, Crewe/ UK) δ13C, δ15N, δ34S, C%, N%, S% in natural solid samples (plants, soils and animal tissues) and precipitated or extracted sulphates and sulphites (for example, from water samples).
Picarro Cavity Ring-down Spectrometer L2140-i
With ChemCorrect software and microcombustion unit - high resolution δ2H, δ18O and δ17O of liquid and vapour water samples.
Picarro Cavity Ring-down Spectrometer L2130-i
With ChemCorrect software δ2H and δ18O of liquid and vapour water samples.
Delta XL Isotope Ratio Mass Spectrometer (Thermo/Germany) connected with:
- GasBench II (GB) δ13C and δ18O in carbonates, δ13C in DIC (Dissolved Inorganic Carbon), δ13C in CO2
- Thermal Conversion /Elemental Analyser (TC/EA) δ18O in organic materials, phosphates, sulphates and nitrates.
HORIBA Aqualog Fluorometer
Combined UV/Vis spectrometer and Fluorometer allowing rapid simultaneous measurement of both absorbance spectra and fluorescence Excitation-Emission Matrices.
- Specifically designed for natural organic matter analysis
- Wavelength range: Ex = 200 - 800nm, Em = 250 - 800nm
- Software support with Eigenvector SOLO package for in-house component decomposition by PARAFAC analysis. Direct EEM export to MATLAB toolkits DOMFluor and DrEEM
Additional major devices and equipment
Ball mills for sample grinding and homogenisation.
Freeze-dryer: Virtis Benchtop 2K.
Microbalances: Sartorius MC210S (0.01mg) Mettler Toledo X6T (0.001 mg).
Vacuum line for cryogenic extraction of water from soil and plant samples.
Equilibration method for analysis of water from soils and small biological samples.
Delta V Plus Isotope Ratio Mass Spectrometer (Thermo /Germany) connected with:
- Thermo Elemental Analyser Flush 1112 via Conflo IV δ13C, δ15N, C%, N%, in natural solid samples (plants, soils and animal tissues) and precipitated or extracted sugars, cellulose, nitrates and other compounds.
- Finnigan LC-IsoLink δ13C in DOC (Dissolved Organic Carbon) in water extracts and pre-concentrated water samples.